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Xu, D. Wu, J. Am. Chem. Soc. 124, 7672 (2002) 12 77. Y. Zhi, Y. C. Tang, S. Honda, K. Sato, H. Kuwahara, D. Golberg, Angew. Chem. Int. Ed. 44, 7932 (2005) 12 78. L. Rapoport, Y. Bilik, Y. Feldman, M. R. Cohen, R. Tenne, Nature 387, 791 (1997) 12 79. J. -L. Li, Q. Xu, K. Tanaka, Chem Commun. 16, 1722 (2002) 12 80. C. Tang, Y. Bando, T. Sato, K. , Chem Commun. 1722 (2002) 8 81. M. Nath, A. R. Rao, Adv. Mater. jp Abstract Titanium oxide nanotube (TiO2 nanotube, TNT) is synthesized by the low-temperature solution chemical method via the self-organization to form unique open-end nanotubular morphology with typically 8–10 and 5–7nm in outer and inner diameters, respectively.

Reprinted with permission from [31] TiO2 nanotube with an anatase structure as its base crystal structures at around 400◦ C. Detailed structure analyses have been carried out extensively. Chen et al. [31] investigated the structure of chemically prepared TNT by using highresolution transmission electron microscopy and reported that the TNT was titanate with the chemical formula of H2 Ti3 O7 and proposed the structure model as shown in Fig. 5. On the other hand, Ma et al. [32, 33] showed it was lepidocrocite which was one of the defect-containing titanate with the formula of Hx Ti2−x/4 x/4 O4 .

Yanagida, Phys. Chem. Chem. Phys. 7, 4157–4163 (2005). 26, 30 44. K. Inumaru, T. Kasahara, M. Yasui, S. Yamanaka, Chem. Commun. 16, 2131– 2133 (2005). 28 45. T. Sekino, T. Okamoto, T. Kasuga, T. Kusunose, T. Nakayama, K. Niihara, Key Eng. Mater. 317–318, 251–254 (2006). 28 46. H. Tokudome, A. Shimai, Y. Mitsuya, Y. Tsuru, M. Miyauchi, Mater. Integration, 18(1), 31–35 (2005). (in Japanese) 30 47. H. Tokudome, M. Miyauchi, Chem. Lett. 33, 1108–1109 (2004) 30 48. T. Kasuga, Mater. Integration 18(1), 26–30 (2005).

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